Gas Selection
Table 36
with capillary columns, GC detectors require a separate makeup gas for
optimum sensitivity. The MSD uses GC carrier gas.
If using any MS system, use of hydrogen as the carrier gas may require
hardware modifications for best performance. Contact your Agilent service
representative.
Nitrogen and Argon/Methane are generally not suitable for GC/MS carrier gas.
N O T E
Table 36
Gases usable with Agilent GCs and capillary columns
Detector type
Electron capture (ECD)
Flame ionization (FID)
Flame photometric (FPD)
Thermal conductivity
(TCD)
Table 37
makeup gases are not required with packed columns.
GC, GC/MS, and ALS Site Preparation Guide
lists gases usable with Agilent GCs and capillary columns. When used
Carrier
Preferred makeup
Hydrogen
Nitrogen
Helium
Nitrogen
Argon/Methane (5%)
Hydrogen
Nitrogen
Helium
Nitrogen
Nitrogen
Nitrogen
Hydrogen
Nitrogen
Helium
Nitrogen
Nitrogen
Nitrogen
Argon
Nitrogen
Hydrogen
Must be same as
Helium
carrier and reference
Nitrogen
lists gas recommendations for packed column use. In general,
6850 Series GC Site Preparation
Alternate choice
Detector, anode
purge, or reference
Nitrogen
Anode purge must
Nitrogen
be same as makeup
Argon/Methane (5%)
Nitrogen
Helium
Hydrogen and air for
Helium
detector
Helium
Hydrogen and air for
detector
Must be same as
Reference must be
carrier and reference
same as carrier and
makeup
81