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Agilent GC, GC/MS, and
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Site Preparation Guide
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Inhaltszusammenfassung für Agilent Technologies ALS

  • Seite 1 Agilent GC, GC/MS, and Site Preparation Guide Agilent Technologies...
  • Seite 2 上海市浦东新区外高桥保税区 understood and met. 英伦路 412 号 联系电话： （800）820 3278 Acknowledgments Microsoft and Windows are U.S. registered trademarks of Microsoft Corporation. Intel and Pentium are U.S. registered trade- marks of Intel Corporation. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 3: Inhaltsverzeichnis

    GC/MS Gas and Reagent Requirements Gas Plumbing Supply tubing for most carrier and detector gases Supply tubing for hydrogen gas Two-stage pressure regulators Pressure regulator-gas supply tubing connections Filters and traps Cryogenic Cooling Requirements Using carbon dioxide GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 4 Supply tubing for most carrier and detector gases Supply tubing for hydrogen gas Two-stage pressure regulators Pressure regulator-gas supply tubing connections Filters and traps Cryogenic Cooling Requirements Using carbon dioxide Maximum Length of Cables GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 5 Requirements for hydrogen as a carrier gas GC/MS Gas and Reagent Requirements Gas Plumbing Supply tubing for most carrier and detector gases Supply tubing for hydrogen gas Two-stage pressure regulators Pressure regulator-gas supply tubing connections Filters and traps GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 6 Maximum Length of Cables Site LAN Network PC Requirements 7693A and 7650 Automatic Liquid Sampler Site Preparation Customer Responsibilities Basic Tools and Consumable Supplies Dimensions and Weight Power Consumption Environmental Conditions Chiller Supplies GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 7: Agilent Technologies

    PC Requirements This section outlines the space and resource requirements for GC, GC/MS, and automatic liquid sampler (ALS) installation. For a successful and timely installation of the instrument, the site must meet these requirements before beginning installation. Necessary supplies (gases, tubing, operating supplies, consumables, and other usage-dependent items such as columns, vials, syringes, and solvents) must also be available.

  • Seite 8: Customer Responsibilities

    If Agilent is delivering installation and familiarization services, delays due to inadequate site preparation could cause loss of instrument use during the warranty period. In extreme cases, Agilent Technologies may ask to be reimbursed for the additional time required to complete the installation.

  • Seite 9: Installation Kits

    1 moisture, and 2 charcoal filters), 1/8-inch brass nuts and ferrules, copper tubing, 1/8-inch brass tees, tubing cutter, 1/8-inch brass caps, universal external split vent trap with replacement cartridges, and 1/8-inch ball valve GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 10 Swagelok fitting needed to connect to the instrument. These fittings are not included with the GC. These fittings are not included with the installation kits. See “Gas Plumbing” on page 43 for part information. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 11: Hydrogen Gas

    See “Exhaust Venting” on page 25. • When using hydrogen carrier gas, also plan to safely vent inlet split vent flows and purge vent flows. See “Exhaust Venting” on page 25. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 12: Dimensions And Weight

    30 cm (12 in) 54 cm (22 in) 41 kg (90 lb) • Performance CI/EI turbo pump 41 cm (16 in) 30 cm (12 in) 54 cm (22 in) 46 kg (100 lb) GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 13 3.9 kg (8,6 lb) each • GC with 7693A ALS tray Requires 43 cm (16.8 in) left of the GC 6.8 kg (15 lb) Requires 4.2 cm (1.7 inch) in front of GC each GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 14 3.0 kg (7 lb) A system that includes a 7890 Series GC, a 5977, 5975, 7010 or 7000 MS, an ALS, and a computer would require about 168 cm (5.5 ft) of bench space (see Figure 1). A 7890 Series system with a GC, Ion Trap MS, ALS, and computer would require about 206 cm (6.7 ft) of bench space (or 148 cm [4.8 ft]...
  • Seite 15 Depth: 92 cm (3 ft) Figure 1 Front view of example installation, 7890B GC/5977 MSD system with 7693A ALS. Note that GC and ALS bench space requirements are the same, with or without an MSD. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 16 168 cm (5.5 ft) Figure 2 Front view of example installation, 7890A GC/7010 system with 7693A ALS. Note that GC and ALS bench space requirements are the same, with or without an MSD. A 7890 Series system that includes a GC, a Q-TOF MS, an ALS, and a computer would require about 197 cm (6.5 ft) of bench space that is at least 92 cm (3 ft)
  • Seite 17 197 cm (6.5 ft) Figure 3 Front view of example installation. 7890B GC/7250 Q-TOF MS system with 7693A ALS shown. Note that the length of the quadrupole vacuum hose is 130 cm (4 ft 3 in) from the high vacuum pump to the foreline pump, and the length of the foreline pump power cord is 2 m (6 ft 6 in).
  • Seite 18 66 cm × 206 cm × 81 cm × 87 kg (26 in × 81 in x 32 in × 191 lbs). The 7200 flight tube shipping pallet is 66 cm × 66 cm × 147 cm × 36.4 kg (26 in × 26 in × 58 in × 80 lbs). GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 19: Power Consumption

    50/60 ± 5% 1100 (400 for 10 Amp (–10% / +5%) foreline pump only) Dedicated 5975 Series MSD 220–240 50/60 ± 5% 1100 (400 for 10 Amp (–10% / +5%) foreline pump only) Dedicated GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 20 Table 3. If the voltage option you ordered is not suitable for your installation, contact Agilent Technologies. Note that ALS instruments receive their power from the GC. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 21: Usa Fast Heating Oven, 240 V

    • The circuit breaker for the branch circuit, which is dedicated to the instrument, is rated for continuous operation. • The service box branch circuit is marked as a “Dedicated Circuit.” GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 22: Common Instrument Power Cord Plugs

    Power cord terminations Cable Plug Country Voltage Amps length (m) Termination type Termination Australia AS 3112 China GB 1002 Europe, Korea 220 / 230 / CEE/7/V11 Denmark, Switzerland Swiss/Denmark 1302 India, South Africa AS 3112 GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 23 Israeli SI32 Japan NEMA L6-20P United Kingdom, Hong BS89/13 Kong, Singapore, Malaysia United States 20, 12 AWG NEMA 5-20P United States 15, 14 AWG NEMA L6-15P Taiwan, South America 20, 12 AWG NEMA 5-20P GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 24: Heat Dissipation

    5975 Series MSD 3000 BTU/hour (3165 kJ/h) 5977 Series MSD 3000 BTU/hour (3165 kJ/h) 7010 or 7000 Triple Quad MS 3700 BTU/hour (3904 kJ/h) 7200 or 7250 Q-TOF MS 6200 BTU/hour (6541 kJ/h) GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 25: Exhaust Venting

    65 ft /min (1.840 m /min). Without the deflector, the exhaust rate is about 99 ft /min (2.8 m /min). The deflector outlet diameter is 10 cm (4 in). GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 26: Other Gases

    Appendix B), or the applicable state regulation. For other countries, consult with the appropriate agency for equivalent requirements. Agilent recommends a vent line internal diameter of 6 mm (1/4-inch) or greater. With a line of this diameter, the length is not critical. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 27: Exhaust Vent Fittings

    • TCD, μECD: The detector exhaust terminates in a 1/8-inch od tube. • SS, MMI, PTV, VI: The split vent terminates in a 1/8-inch Swagelok female fitting. • All inlets: The septum purge vent terminates in 1/8-inch od tubing. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 28: Environmental Conditions

    (–4 to 158 °F) 7200 or 7250 Q-TOF MS Operation 15 to 35 °C 20 to 80% 2,500 m (59 to 95 °F) Storage –20 to 70 °C 0 to 95% (–4 to 158 °F) GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 29 1 Operation requires constant temperature (variations < 2 C/hour) 2 Operation requires constant temperature (variations < 2 C/hour) 3 An altitude of 3,700 meters (12,000 feet) is supported if the ambient temperature is less than 30 °C GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 30: Gas And Reagent Selection

    Nitrogen makeup 1 Depending on bead type, higher makeup gas flow rates (> 5 mL/min) may introduce cooling effects or shorten bead life. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 31 1 Slightly greater sensitivity than helium. Incompatible with some compounds. 2 For analysis of hydrogen or helium. Greatly reduces sensitivity for other compounds. For installation checkout, Agilent requires the gas types shown in Table GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 32 Please refer to the Hydrogen Safety Guide shipped with your instrument. Hydrogen use is specifically prohibited with the 7200 or 7250 GC/Q-TOF system. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 33 MS and MSD systems purchased with a Self-Cleaning Ion Source also require a source of hydrogen gas in addition to helium carrier gas. This source can be shared but must meet carrier gas purity requirements. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 34: Gas And Reagent Purity

    3 Required reagent gas for installation and performance verification, external CI MS only. The 5975, 5977, 7000 GC/MS, 7200 Q-TOF MS, and 240 Ion Trap operate in an external CI mode. 4 Optional reagent gases, CI mode only. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 35: Gas Supplies

    Helium, Argon, Nitrogen 125 psig (8.6 Bar) 5183-4644 Table 12 Table 14 list minimum and maximum delivery pressures for inlets and detectors, measured at the bulkhead fittings on the back of the instrument. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 36 Maximum delivery pressures for detectors, at the GC/MS, in kPa (psig) Detector type Hydrogen 240–690 (35–100) 240–690 (35–100) 310–690 (45–100) 380–690 (55–100) 380–690 (55–100) 690–827 (100–120) Makeup 380–690 (55–100) 380–690 (55–100) 380–690 (55–100) 380–690 (55–100) 380–690 (55–100) Reference 380–690 (55–100) GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 37: Hydrogen Supply Requirements For Carrier Gas And Jetclean Systems

    (good) specifications for water and oxygen content. If using a hydrogen gas cylinder, Agilent recommends use of Gas Clean Filters to purify the gas. Consider additional safety equipment as recommended by your company safety personnel. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 38: Gc/Ms Gas And Reagent Requirements

    1 Total gas flow into the MSD = column flow + reagent gas flow (if applicable) + Agilent CFT device flow (if applicable). Instruments using a JetClean ion source system may also add a small (~0.075 mL/min) hydrogen flow. 2 Expect degradation of spectral performance and sensitivity. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 39 1 to 2 (15 to 20 psi) 1 Hydrogen gas can be used for the carrier gas but specifications are based on helium as the carrier gas. Please observe all hydrogen gas safety cautions. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 40 Methane reagent gas 103 to 172 kPa 1 to 2 (required for CI operation) (15 to 25 psi) Ammonia reagent gas (optional) 34 to 55 kPa 1 to 2 (5 to 8 psi) GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 41 0.32 mm (30 m long) 1 Total gas flow into the MS = column flow + reagent gas flow (if applicable) + collision cell gas flow. 2 Expect degradation of spectral performance and sensitivity. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 42 ≤ 621 kPa (90 psi) Hydrogen 1 Any delivery pressure ≤ 621 kPa (90 psi) is acceptable as long as it is 69 kPa (10 psi) higher than the maximum hydrogen pressure needed during operation. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 43: Gas Plumbing

    Main gas supply “Filters and traps” page 47 for more information. Shutoff valve Gas Clean filter configuration will vary depending on the application. Figure 5 Recommended filters and plumbing configuration from a carrier gas cylinder GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 44: Supply Tubing For Most Carrier And Detector Gases

    Supply tubing for most carrier and detector gases Use only preconditioned copper tubing (part number 5180-4196) to supply gases to the instrument. Do not use ordinary copper tubing—it contains oils and contaminants. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 45: Supply Tubing For Hydrogen Gas

    • Especially do not use old copper tubing, which can become brittle. Do not use old copper tubing with hydrogen gas. Old copper tubing can become WA R N I N G brittle and create a safety hazard. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 46: Two-Stage Pressure Regulators

    Agilent catalog for consumables and supplies contains information to help you identify the correct regulator, as determined by the Compressed Gas Association (CGA). Agilent Technologies offers pressure-regulator kits that contain all the materials needed to install regulators properly. Pressure regulator-gas supply tubing connections Use PTFE tape to seal the pipe-thread connection between the pressure regulator outlet and the fitting to which you connect the gas tubing.

  • Seite 47: Filters And Traps

    • Oxygen - Prevents oxidation of the GC column, septum, liner, and glass wool. • Moisture - Delivers fast stabilization times for increased GC productivity, and prevents hydrolization damage to the stationary phase, column, liner, glass wool, or septum in the GC. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 48 • GC/MS - Delivers fast stabilization times for increased GC productivity, removes oxygen, moisture, and hydrocarbons from the carrier gas for MS applications, and provides ultimate GC column protection. Table 25 on page 49 shows recommended filter connection diagrams for common instrument configurations. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 49: Connection Diagram

    (Carrier Gas differs from Make-Up Gas) Hydrogen Charcoal Filter Charcoal Filter Carrier Gas Oxygen Filter Moisture Filter Column Flame Photometric Detector Flame 1 Hydrogen Charcoal Filter PFPD Charcoal Filter Pulsed Flame Photometric Detector Flame 2 GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 50 Table 26 lists the most common Gas Clean Filter system kits. See the Agilent online store or contact your local Agilent sales representative for additional filters, parts, and accessories applicable to your instrument configuration. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 51 ECD, GC/MS tubing, and two 1/8-inch nuts and ferrules) TCD filter kit (with oxygen and moisture filters) CO738408 Each separate gas supply requires its own filters. See also “Installation Kits” on page 9. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 52: Cryogenic Cooling Requirements

    The CO should be free of particulate material, oil, and other contaminants. These contaminants could clog the expansion orifice or affect the proper operation of the GC. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 53 • Do not use a padded tank (one to which another gas is added to increase the pressure). Dip tube Correct configuration Incorrect configuration GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 54: Using Liquid Nitrogen

    • Situate the liquid nitrogen tank close (within 1.5 to 3 m, or 5 to 10 feet) to the GC to ensure that liquid, not gas, is supplied to the inlet. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 55: Using Compressed Air

    Installation of a compressed air line to the inlet cryo coolant valve requires the hardware (and appropriate fittings) noted below: • Use 1/4-inch copper or stainless steel tubing for supply tubing to the N valve GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 56: Maximum Length Of Cables And Hoses

    The length of the vacuum hose is 130 cm (4.24 feet) from the high vacuum pump to the foreline pump, while the length of the foreline pump power cord is 2 meters (6.6 feet). GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 57: Site Lan Network

    If you intend to connect your system to your site’s LAN network, you must have an additional shielded twisted pair network cable (8121-0940). Agilent Technologies is not responsible for connecting to or establishing communication N O T E with your site LAN network. The representative will test the system’s ability to communicate on a mini-hub or LAN switch only.
  • Seite 58 GC/MS hardware and software using the triple NIC configuration, and has no known network configuration issues. Alternate network configurations can be configured and managed by the end user at their own risk and expense. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 59: Pc Requirements

    7890 Series GC Site Preparation PC Requirements If using an Agilent data system, refer to the data system documentation for PC requirements. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 60 7890 Series GC Site Preparation GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 61: Agilent Technologies

    PC Requirements This section outlines the space and resource requirements for GC, GC/MS, and automatic liquid sampler (ALS) installation. For a successful and timely installation of the instrument, the site must meet these requirements before beginning installation. Necessary supplies (gases, tubing, operating supplies, consumables, and other usage-dependent items such as columns, vials, syringes, and solvents) must also be available.

  • Seite 62: Customer Responsibilities

    If Agilent is delivering installation and familiarization services, delays due to inadequate site preparation could cause loss of instrument use during the warranty period. In extreme cases, Agilent Technologies may ask to be reimbursed for the additional time required to complete the installation.

  • Seite 63: Basic Tools And Installation Kits

    Holding GC and MS tools. Q-Tips Cleaning source parts. Cloths Keeping surfaces and parts clean. Gloves Reducing contamination on GC and MSD parts. Funnel Changing oil. Hex key, 5 mm or 8 mm Removing oil plug. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 64 Please refer to the latest Agilent consumables and supplies catalog and to the Agilent web site at www.agilent.com/chem for part numbers and recommended maintenance periods. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 65 These kits are not supplied with the instrument. Agilent highly recommends these kits if you did not order the pre-plumbed option. These kits include tools and hardware required to plumb gases to the GC. See Table GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 66 1 moisture, and 2 charcoal filters), 1/8-inch brass nuts and ferrules, copper tubing, 1/8-inch brass tees, tubing cutter, 1/8-inch brass caps, universal external split vent trap with replacement cartridges, and 1/8-inch ball valve GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 67 (For TCD/ECD , also order an additional Gas Clean Filter CP17974.) Gas Clean Filter kit GC-MS 1/8in.,1/pk CP17974 Gas Clean filter kit with 1/8-inch fittings (order 2 if using separate makeup and carrier gas supplies). GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 68 Swagelok fitting needed to connect to the instrument. These fittings are not included with the GC. These fittings are not included with the installation kits. See “Gas Plumbing” on page 89 for part information. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 69: Hydrogen Carrier Gas

    Uncombusted hydrogen can present a safety hazard. See “Exhaust Venting” on page 79. • When using hydrogen carrier gas, also plan to safely vent inlet split vent flows and purge vent flows. See “Exhaust Venting” on page 79. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 70: Dimensions And Weight

    30 cm (12 in) 54 cm (22 in) 41 kg (90 lb) • Performance CI/EI turbo pump 41 cm (16 in) 30 cm (12 in) 54 cm (22 in) 46 kg (100 lb) GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 71 Requires 4.2 cm (1.7 inch) in front of GC each A 6850 system that includes a GC, an ALS injector, and a computer would require about 138 cm (4 ft 6 in) of bench space. Allowing for operational access and a printer, a total of 229 cm (7.5 ft) of bench space should be available for a full GC/MS system.
  • Seite 72 Note that the length of the quadrupole vacuum hose is 130 cm (4 ft 3 in) from the high vacuum pump to the foreline pump, and the length of the foreline pump power cord is 2 m (6 ft 6 in). GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 73: Power Consumption

    6850 Series GC Fast 200/208 48–63 2400 15 Amp single/split phase Dedicated (–10% / +10%) 5975 Series MSD 50/60 ± 5% 1100 (400 for 10 Amp (–10% / +5%) foreline pump only) Dedicated GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 74 32. If the voltage option you ordered is not suitable for your installation, contact Agilent Technologies. Note that ALS instruments receive their power from the GC. A proper earth ground is required for GC operations. Any interruption of the grounding...

  • Seite 75: Canadian Installation

    • The service box branch circuit is marked as a “Dedicated Circuit.” Common instrument power cord plugs Table 33 below shows common Agilent power cord plugs. Table 33 Power cord terminations Cable Plug Country Voltage Amps length (m) Wall termination Termination Australia AS 3112 GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 76 (m) Wall termination Termination China GB 1002 Europe, Korea 220 / 230 / CEE/7/V11 Denmark, Switzerland Swiss/Denmark 1302 India, South Africa AS 3112 Israel 16, 16 AWG Israeli SI32 Japan NEMA L6-20P GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 77 (m) Wall termination Termination United Kingdom, Hong BS89/13 Kong, Singapore, Malaysia United States 20, 12 AWG NEMA 5-20P United States 15, 14 AWG NEMA L6-15P Taiwan, South America 20, 12 AWG NEMA 5-20P GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 78: Heat Dissipation

    < 4800 BTU/hour maximum (< 5064 kJ/h) < 4800 BTU/hour maximum (< 5064 kJ/h) 6850 Series GC Steady state, including MS interface 5975 Series MSD 3000 BTU/hour (3165 kJ/h) 5977 Series MSD 3000 BTU/hour (3165 kJ/h) GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 79: Exhaust Venting

    Note that an exhaust vent system is not part of the building environmental control system, which recirculates air. Exhaust venting must comply with all local environmental and safety codes. Contact your Environmental Health & Safety (EHS) specialist. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 80: Environmental Conditions

    15 to 35 °C 20 to 80% 4,615 m (59 to 95 °F) Storage –20 to 70 °C 0 to 95% (–4 to 158 °F) 1 Operation requires constant temperature (variations < 2 C/hour) GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 81: Gas Selection

    (TCD) Helium carrier and reference carrier and reference same as carrier and Nitrogen makeup Table 37 lists gas recommendations for packed column use. In general, makeup gases are not required with packed columns. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 82 1 Slightly greater sensitivity than helium. Incompatible with some compounds. 2 For analysis of hydrogen or helium. Greatly reduces sensitivity for other compounds. For installation checkout, Agilent requires the gas types shown in Table GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 83 Always turn off the hydrogen supply at its source before working on the instrument. Please refer to the Hydrogen Safety Guide shipped with your instrument. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 84: Gas And Reagent Purity

    2 Required reagent gas for installation and performance verification, external CI MS only. The 5975 and 5977 operate in an external CI mode.. 3 Optional reagent gases, CI mode only. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 85: Gas Supplies

    Delivery pressures for inlets required at the GC/MS, in kPa (psig) Inlet type Split/Splitless 150 psi Split/Splitless 100 psi On-column Purged packed Carrier (max) 1,172 (170) 827 (120) 827 (120) 827 (120) 827 (120) Carrier (min) (20 psi) above pressure used in method GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 86: Requirements For Hydrogen As A Carrier Gas

    (good) specifications for water and oxygen content. If using a hydrogen gas cylinder, Agilent recommends use of Gas Clean Filters to purify the gas. Consider additional safety equipment as recommended by your company safety personnel. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 87: Gc/Ms Gas Requirements

    0.53 mm (30 m) 1 Total gas flow into the MSD = column flow + reagent gas flow (if applicable) + Agilent CFT device flow (if applicable). 2 Expect degradation of spectral performance and sensitivity. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 88 1 to 2 (15 to 20 psi) 1 Hydrogen gas can be used for the carrier gas but specifications are based on helium as the carrier gas. Please observe all hydrogen gas safety cautions. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 89: Gas Plumbing

    Main gas supply “Filters and traps” page 93 for more information. Shutoff valve Gas Clean filter configuration will vary depending on the application. Figure 7 Recommended filters and plumbing configuration from a carrier gas cylinder GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 90: Supply Tubing For Most Carrier And Detector Gases

    Supply tubing for most carrier and detector gases Use only preconditioned copper tubing (part number 5180-4196) to supply gases to the instrument. Do not use ordinary copper tubing—it contains oils and contaminants. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 91: Supply Tubing For Hydrogen Gas

    • Especially do not use old copper tubing, which can become brittle. Do not use old copper tubing with hydrogen gas. Old copper tubing can become WA R N I N G brittle and create a safety hazard. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 92: Two-Stage Pressure Regulators

    Agilent catalog for consumables and supplies contains information to help you identify the correct regulator, as determined by the Compressed Gas Association (CGA). Agilent Technologies offers pressure-regulator kits that contain all the materials needed to install regulators properly. Pressure regulator-gas supply tubing connections Use PTFE tape to seal the pipe-thread connection between the pressure regulator outlet and the fitting to which you connect the gas tubing.

  • Seite 93: Filters And Traps

    • Oxygen - Prevents oxidation of the GC column, septum, liner, and glass wool. • Moisture - Delivers fast stabilization times for increased GC productivity, and prevents hydrolization damage to the stationary phase, column, liner, glass wool, or septum in the GC. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 94 • GC/MS - Delivers fast stabilization times for increased GC productivity, removes oxygen, moisture, and hydrocarbons from the carrier gas for MS applications, and provides ultimate GC column protection. Table 47 on page 95 shows recommended filter connection diagrams for common instrument configurations. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 95: Connection Diagram

    Make-Up Gas Charcoal Filter (Carrier Gas differs from Make-Up Gas) Hydrogen Charcoal Filter Charcoal Filter Carrier Gas Oxygen Filter Moisture Filter Column Flame Photometric Detector Flame 1 Hydrogen Charcoal Filter Charcoal Filter Flame 2 GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 96 Table 48 lists the most common Gas Clean Filter system kits. See the Agilent online store or contact your local Agilent sales representative for additional filters, parts, and accessories applicable to your instrument configuration. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 97 1/8-inch nuts and ferrules) TCD filter kit (with oxygen and moisture filters) CO738408 Each separate gas supply requires its own filters. See also “Basic Tools and Installation Kits” on page 63. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 98: Cryogenic Cooling Requirements

    25 °C. • Use 1/8-inch diameter heavy-wall stainless steel tubing for supply tubing. The tubing should be between 1.5 and 15 m (5 and 50 feet) long. (Agilent part number 7157-0210, 20 ft) GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 99 • Do not use a padded tank (one to which another gas is added to increase the pressure). Dip tube Correct configuration Incorrect configuration GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 100: Maximum Length Of Cables

    130 cm (4.24 feet) from the high vacuum pump to the foreline pump, while the length of the foreline pump power cord is 2 meters (6.6 feet). GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 101: Site Lan Network

    If you intend to connect your system to your site’s LAN network, you must have an additional shielded twisted pair network cable (8121-0940). Agilent Technologies is not responsible for connecting to or establishing communication N O T E with your site LAN network. The representative will test the system’s ability to communicate on a mini-hub or LAN switch only.

  • Seite 102: Pc Requirements

    6850 Series GC Site Preparation PC Requirements If using an Agilent data system, refer to the data system documentation for PC requirements. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 103: Agilent Technologies

    Note that performance verification requires the use of helium carrier gas.Refer to the Agilent Web site at www.agilent.com/chem the most up-to-date listing of GC and ALS supplies and consumables. For a general 7820A GC-only installation, refer to its documentation. Agilent Technologies...

  • Seite 104: Customer Responsibilities

    If Agilent is delivering installation and familiarization services, delays due to inadequate site preparation could cause loss of instrument use during the warranty period. In extreme cases, Agilent Technologies may ask to be reimbursed for the additional time required to complete the installation.

  • Seite 105: Agilent Technologies Installation And Familiarization Services

    • Familiarization or installation of non-Agilent software To arrange for additional services, including training or application development, contact your Agilent sales representative or visit the Agilent web site at www.agilent.com/chem. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 106: Basic Tools And Consumable Supplies

    Verifying flows, checking for leaks and plugs Electronic gas leak detector (G3388B) Locating gas leaks; safety checks when using Hydrogen Electronic vial crimper Assuring consistently air-tight vial closure, regardless of who does the crimping GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 107 Inlet preventative maintenance (PM) kits Kits with individual parts needed to maintain an inlet Pneumatic supplies Gases, traps, o-rings, seals, Swagelok fittings Column supplies Nuts, ferrules, adapters, guard columns, retention gaps Application supplies Standards, columns, syringes GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 108: Dimensions And Weight

    • GC/MS operational and maintenance access Requires 30 cm (1 ft) to its left • GC with 7693A ALS injector Requires 50 cm (19.5 in) above the GC 3.9 kg (8,6 lb) each GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 109 Requires 30 cm (12 in) left of the GC 3.0 kg (7 lb) A 7820 MSD system that includes a GC, ALS injector, 5977 or 5975 MSD and a computer would require about 165 cm (5 ft 5 in.) of bench space. Some repairs to the GC will also require access to the back of the instrument.

  • Seite 110: Power Consumption

    50/60 ± 5% 1100 (400 for 10 Amp (–10% / +5%) foreline pump only) Dedicated 5977 Series MSD 50/60 ± 5% 1100 (400 for 10 Amp (–10% / +5%) foreline pump only) Dedicated GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 111: Grounding

    27. If the voltage option you ordered is not suitable for your installation, contact Agilent Technologies. Note that ALS instruments receive their power from the GC. Grounding A proper earth ground is required for GC operations. Any interruption of the grounding...

  • Seite 112: Canadian Installation

    Common instrument power cord plugs Table 54 below shows common Agilent power cord plugs. Table 54 Power cord terminations Cable Plug Country Voltage Amps length (m) Termination type Termination Australia AS 3112 China GB 1002 GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 113 Europe, Korea 220 / 230 / CEE/7/V11 Denmark, Switzerland Swiss/Denmark 1302 India, South Africa AS 3112 Japan NEMA L6-20P United Kingdom, Hong BS89/13 Kong, Singapore, Malaysia United States 20, 12 AWG NEMA 5-20P GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 114 7820 MSD Site Preparation Table 54 Power cord terminations (continued) Cable Plug Country Voltage Amps length (m) Termination type Termination United States 15, 14 AWG NEMA L6-15P Taiwan, South America 20, 12 AWG NEMA 5-20P GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 115: Heat Dissipation

    Standard heater ramp 7820A GC 7681 BTU/hour maximum (8103 kJ/h) 5120 BTU/hour maximum (100 V power option) (5402 kJ/h) 5975 Series MSD 3000 BTU/hour (3165 kJ/h) 5977 Series MSD 3000 BTU/hour (3165 kJ/h) GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 116: Exhaust Venting

    Appendix B), or the applicable state regulation. For other countries, consult with the appropriate agency for equivalent requirements. Agilent recommends a vent line internal diameter of 6 mm (1/4-inch) or greater. With a line of this diameter, the length is not critical. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 117: Exhaust Vent Fittings

    The various inlet and detector vents terminate in the following fittings: • TCD, μECD: The detector exhaust terminates in a 1/8-inch od tube. • All inlets: The septum purge vent terminates in 1/8-inch od tubing. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 118: Environmental Conditions

    15 to 35 °C 20 to 80% 4,615 m (59 to 95 °F) Storage –20 to 70 °C 0 to 95% (–4 to 158 °F) * Operation requires constant temperature (variations < 2 C/hour) GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 119: Gas And Reagent Selection

    Always turn off the hydrogen supply at its source before working on the instrument. Please refer to the Hydrogen Safety Guide shipped with your instrument. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 120: Gas And Reagent Purity

    Always turn off the hydrogen supply at its source before working on the instrument. Please refer to the Hydrogen Safety Guide shipped with your instrument. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 121: Gas Supplies

    Helium, Argon, Nitrogen 125 psig (8.6 Bar) 5183-4644 Table 59 Table 60 list minimum and maximum delivery pressures for inlets and detectors, measured at the bulkhead fittings on the back of the instrument. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 122: Requirements For Hydrogen As A Carrier Gas

    (good) specifications for water and oxygen content. If using a hydrogen gas cylinder, Agilent recommends use of Gas Clean Filters to purify the gas. Consider additional safety equipment as recommended by your company safety personnel. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 123: Gc/Ms Gas And Reagent Requirements

    * Total gas flow into the MSD = column flow + reagent gas flow (if applicable) + Agilent CFT device flow (if applicable). Instru- ments using a JetClean ion source system may also add a small (~0.075 mL/min) hydrogen flow. † Expect degradation of spectral performance and sensitivity. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 124 (column and split flow) (50 to 80 psi) * Hydrogen gas can be used for the carrier gas but specifications are based on helium as the carrier gas. Please observe all hydrogen gas safety cautions. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 125: Gas Plumbing

    Main gas supply “Filters and traps” page 129 for more information. Shutoff valve Gas Clean filter configuration will vary depending on the application. Figure 9 Recommended filters and plumbing configuration from a carrier gas cylinder GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 126: Supply Tubing For Most Carrier And Detector Gases

    • Never use chlorinated solvents to clean tubing or fittings. Supply tubing for most carrier and detector gases Use only preconditioned copper tubing (part number 5180-4196) to supply gases to the instrument. Do not use ordinary copper tubing—it contains oils and contaminants. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 127: Supply Tubing For Hydrogen Gas

    • Especially do not use old copper tubing, which can become brittle. Do not use old copper tubing with hydrogen gas. Old copper tubing can become WA R N I N G brittle and create a safety hazard. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 128: Two-Stage Pressure Regulators

    Agilent catalog for consumables and supplies contains information to help you identify the correct regulator, as determined by the Compressed Gas Association (CGA). Agilent Technologies offers pressure-regulator kits that contain all the materials needed to install regulators properly. Pressure regulator-gas supply tubing connections Use PTFE tape to seal the pipe-thread connection between the pressure regulator outlet and the fitting to which you connect the gas tubing.

  • Seite 129: Filters And Traps

    • Oxygen - Prevents oxidation of the GC column, septum, liner, and glass wool. • Moisture - Delivers fast stabilization times for increased GC productivity, and prevents hydrolization damage to the stationary phase, column, liner, glass wool, or septum in the GC. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 130 • GC/MS - Delivers fast stabilization times for increased GC productivity, removes oxygen, moisture, and hydrocarbons from the carrier gas for MS applications, and provides ultimate GC column protection. Table 65 on page 131 shows recommended filter connection diagrams for common instrument configurations. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 131: Connection Diagram

    Make-Up Gas Charcoal Filter (Carrier Gas differs from Make-Up Gas) Hydrogen Charcoal Filter Charcoal Filter Carrier Gas Oxygen Filter Moisture Filter Column Flame Photometric Detector Flame 1 Hydrogen Charcoal Filter Charcoal Filter Flame 2 GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 132 Table 66 lists the most common Gas Clean Filter system kits. See the Agilent online store or contact your local Agilent sales representative for additional filters, parts, and accessories applicable to your instrument configuration. GC, GC/MS, and ALS Site Preparation Guide...
  • Seite 133 GC/MS Gas Clean Filter installation kit (includes CP17976, 1 m copper CP17978 ECD, GC/MS tubing, and two 1/8-inch nuts and ferrules) TCD filter kit (with oxygen and moisture filters) CO738408 Each separate gas supply requires its own filters. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 134: Maximum Length Of Cables

    • The length of the Agilent-supplied remote cable is 2 meters (6.6 feet). • The length of the Agilent-supplied LAN cable is 10 meters (32.8 feet). • The lengths of the power cords are 2 meters (6.6 feet). GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 135: Site Lan Network

    If you intend to connect your system to your site’s LAN network, you must have an additional shielded twisted pair network cable (8121-0940). Agilent Technologies is not responsible for connecting to or establishing communication N O T E with your site LAN network. The representative will test the system’s ability to communicate on a mini-hub or LAN switch only.

  • Seite 136: Pc Requirements

    7820 MSD Site Preparation PC Requirements Any 7820 GC/MSD system requires Agilent control software. For PC requirements, refer to the Agilent data system documentation. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 137: 7693A And 7650 Automatic Liquid Sampler Site Preparation

    Refer to the Agilent Web site at www.agilent.com/chem for the most up-to-date listing of GC, GC/MS, and ALS supplies and consumables. Refer to your GC documentation for compatibility with a specific ALS model. Agilent Technologies...

  • Seite 138: Customer Responsibilities

    If Agilent is delivering installation and familiarization services, delays due to inadequate site preparation could cause loss of instrument use during the warranty period. In extreme cases, Agilent Technologies may ask to be reimbursed for the additional time required to complete the installation.

  • Seite 139: Basic Tools And Consumable Supplies

    7693A and 7650 Automatic Liquid Sampler Site Preparation Basic Tools and Consumable Supplies The 7693A and 7650 ALS come with a few basic tools and consumables depending on the hardware that you ordered. Below is a general list of what comes with the instrument.

  • Seite 140: Dimensions And Weight

    Requires 9 cm (3.6 in) in front of the GC Requires 3 cm (1.2 in) to the left of the GC 1 The G4520A Tray with a bar code reader is available with a G4514A Tray and G4515A bar code reader. GC, GC/MS, and ALS Site Preparation Guide...

  • Seite 141: Power Consumption

    7693A and 7650 Automatic Liquid Sampler Site Preparation Power Consumption The ALS components draw power from the GC. No other power source is required. Environmental Conditions Operating the instrument within the recommended ranges optimizes instrument performance and lifetime. The sampler system operates in the same environment as its parent GC.

  • Seite 142: Chiller Supplies

    Agilent Technologies Chiller Supplies If using the optional G4522A Cooling Accessory, you will need to supply: • A water chiller • Tubing and 1/8-inch Swagelok fittings to connect the chilled water and return water to the chiller • A container or drain to dispose of condensate from the tray...

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