Shimadzu LCMS-8045 CL Benutzerhandbuch Seite 143

### Sample Information ###
Sample Type: PEG+PPG+Raffinose
### Tuning Condition ###
Detector Adjustment: On
Resolution Adjustment: On
FWHM of Spectrum: 0.70
Sensitivity Adjustment: On
Mass Calibration: On
### Tuning Result ###
Model: LCMS-8045
Interface: DUIS
Polarity: Pos
Tuning Mode: Auto
Tuning Date: 5/17/2017 11:13:39 AM
Acquisition Mode: Product Scan
Nebulizing Gas Flow: 1.50(settings : 1.50) L/min
Drying Gas Flow: 0.00(settings : 10.00) L/min
### Tuning Profile ###
CD:-10.00 kV CD:-10.00 kV CD:-10.00 kV
Int.: 236412 Int.: 210232
FWHM: 0.74 FWHM: 0.73
m/z : 45.05 m/z : 89.05
Pre m/z: 388.25 Pre m/z: 388.25 Pre m/z: 388.25
Mag.: 83 Mag.: 92
Scan Range: 2.00 - 438.25 Scan Speed: 30 u/s Base Peak: 371.20 (1042664) Pre m/z: 388.25
100
45.05 89.05 133.10 177.10
100 200
m/z(Target) m/z(Actual) Difference
388.25 > 45.05 45.05
388.25 > 89.05 89.05
388.25 > 133.10 133.10
388.25 > 177.10 177.10
Const 65.05
DL Bias Const +0.0 +0.0
Qarray Bias Const +0.0 +0.0
Qarray RF Scan +50.0 +19.3
Multipole RF Scan +100.0 +30.0
Multipole1 Bias Const +0.0 +0.0
Multipole1 Lens Const -0.8
Multipole2 Bias Const -0.8
Multipole2 Lens Const -1.0
Q1 Bias Const -3.5
CC Lens1 Const +0.0 +0.0
CC Lens2 Const -100.0 -100.0
CC Lens3 Const -20.0 -20.0
Const 45.05
CC RF Scan +100.0 +100.0
CE Scan -20.0 -25.0
Q3 Bias Scan -7.0
Const 107.15 1071.50 1893.40
Q1 Pre Bias Scan -15.0
Q3 Pre Bias Scan -15.0
CID Gas Flow:
Heating Gas Flow:
Interface Bias:
Interface Current:
Interface Temp.:
DL Temp.:
Heat Block Temp.:
Q1 RF Gain:
Q1 RF Offset:
Q3 RF Gain:
Q3 RF Offset:
Q1 Post-rod Bias:
CID CELL Exit Lens:
Conversion Dynode:
Detector:
PG Vacuum:
IG Vacuum:
Corona Needle Voltage:
Corona Needle Current:
CD:-10.00 kV
Int.: 284641 Int.: 167521
FWHM: 0.70 FWHM: 0.69
m/z : 133.10 m/z : 177.10
Pre m/z: 388.25
Mag.: 68 Mag.: 115
300 400 500
Width Intensity
0.00 0.74 236412
0.00 0.73 210232
0.00 0.70 284641
0.00 0.69 167521
168.10 256.15 344.20 652.40 1004.60 1893.40
+0.0 +0.0 +0.0 +0.0
+0.0 +0.0 +0.0 +0.0
+50.0 +90.0 +90.0 +130.0
+50.0 +50.0 +50.0 +300.0
+0.0 +0.0 +0.0 +0.0
-0.8 -0.8 -0.8 -0.8 -0.8
-0.8 -0.8 -0.8 -0.8 -0.8
-1.0 -1.0 -1.0 -1.0 -1.0
-3.5 -3.5 -3.5 -3.5 -3.5
+0.0 +0.0 +0.0 +0.0
-100.0 -100.0 -100.0 -100.0
-20.0 -20.0 -20.0 -20.0
89.05 133.10 168.10 1893.40
+120.0 +300.0 +300.0 +300.0
-15.0 -15.0 -15.0 -15.0
-7.0 -7.0 -7.0 -7.0 -9.0
-5.0 -50.0 -50.0
-5.0 -50.0 -50.0
230(settings : 230) kPa
5.02(settings : 5.00) L/Min
+4.00 kV
0.95 uA
100(settings : 100) C
249(settings : 250) C
399(settings : 400) C
4997
4970
4998
5002
-5.0 V
-1.7 V
-10.00 kV
-2.28(-2.28) kV
7.2e+001 Pa
2.1e-003 Pa
+4.50 kV
0.10 uA
600 700 800
+0.0 +0.0
+0.0 +0.0
+130.0 +130.0
+300.0 +300.0
+0.0 +0.0
-0.8 -0.8
-0.8 -0.8
-1.0 -1.0
-3.5 -3.5
+0.0 +0.0
-100.0 -100.0
-20.0 -20.0
LCMS-8045
3.8 Auto-Tuning
3
900
99
LCMS-8050
CL CL