Shimadzu LCMS-8045 CL Benutzerhandbuch Seite 142

3 Vorbereitung
### Sample Information ###
Sample Type:
### Tuning Condition ###
Detector Adjustment:
Resolution Adjustment:
FWHM of Spectrum:
Sensitivity Adjustment:
Mass Calibration:
### Tuning Result ###
Model:
Interface:
Polarity:
Tuning Mode:
Tuning Date:
Acquisition Mode:
Nebulizing Gas Flow:
Drying Gas Flow:
### Tuning Profile ###
CD:+3.00 kV
Int.: 11894411
FWHM: 0.71
m/z : 503.15
Mag.: 1
Scan Range: 2.00 - 2000.00 Scan Speed: 30 u/s Base Peak: 503.15 (20000000)
100
100
m/z(Target)
503.15
1007.30
DL Bias
Qarray Bias
Qarray RF
Multipole RF
Multipole1 Bias
Multipole1 Lens
Multipole2 Bias
Multipole2 Lens
Q1 Bias
CC Lens1
CC Lens2
CC Lens3
CC RF
CE
Q3 Bias
Q1 Pre Bias
Q3 Pre Bias
98
LCMS-8045 LCMS-8050
CL
PEG+PPG+Raffinose
On
On
0.70
On
On
LCMS-8045
DUIS
Neg
Auto
5/17/2017 11:09:36 AM
Q3 Scan(Use CID Gas)
1.50(settings : 1.50) L/min
0.00(settings : 10.00) L/min
CD:+5.00 kV
Int.: 1749183
FWHM: 0.69
m/z : 1007.30
Mag.: 11
503.15
300 500 700
m/z(Actual) Difference Width
503.15 0.00 0.71
1007.30 0.00 0.69
Const 65.05 168.10
Const +0.0 +0.0 +0.0
Const +0.0 +0.0 +0.0
Scan +50.0 +19.3 +50.0
Scan +100.0 +30.0 +50.0
Const +0.0 +0.0 +0.0
Const +0.8 +0.8 +0.8
Const +0.8 +0.8 +0.8
Const +1.0 +1.0 +1.0
Const +3.5 +5.0 +5.0
Const +0.0 +0.0 +0.0
Const +100.0 +100.0 +100.0
Const +20.0 +20.0 +20.0
Const 65.05 168.10
Scan +200.0 +70.0 +110.0
Scan +5.0 +5.0 +5.0
Scan +7.0 +7.0 +7.0
Const 107.15 1071.50 1893.40
Scan +15.0 +5.0 +50.0
Scan +15.0 +5.0 +50.0
CL
CID Gas Flow:
Heating Gas Flow:
Interface Bias:
Interface Current:
Interface Temp.:
DL Temp.:
Heat Block Temp.:
Q1 RF Gain:
Q1 RF Offset:
Q3 RF Gain:
Q3 RF Offset:
Q1 Post-rod Bias:
CID CELL Exit Lens:
Conversion Dynode:
Detector:
PG Vacuum:
IG Vacuum:
Corona Needle Voltage:
Corona Needle Current:
1007.30
900 1100
Intensity
11894411
1749183
256.15 344.20 652.40 1004.60 1893.40
+0.0 +0.0 +0.0 +0.0
+0.0 +0.0 +0.0 +0.0
+90.0 +90.0 +130.0 +130.0 +130.0
+50.0 +50.0 +300.0 +300.0 +300.0
+0.0 +0.0 +0.0 +0.0
+0.8 +0.8 +0.8 +0.8
+0.8 +0.8 +0.8 +0.8
+1.0 +1.0 +1.0 +1.0
+5.0 +5.0 +5.0 +5.0
+0.0 +0.0 +0.0 +0.0
+100.0 +100.0 +100.0 +100.0 +100.0
+20.0 +20.0 +20.0 +20.0 +20.0
256.15 344.20 652.40 1004.60 1893.40
+130.0 +300.0 +300.0 +300.0 +300.0
+5.0 +5.0 +5.0 +5.0
+7.1 +7.2 +7.6 +8.0
+50.0
+50.0
230(settings : 230) kPa
5.01(settings : 5.00) L/Min
-3.00 kV
0.73 uA
100(settings : 100) C
250(settings : 250) C
400(settings : 400) C
---
---
4999
5000
5.0 V
3.5 V
+10.00 kV
-2.28(-2.28) kV
7.2e+001 Pa
2.1e-003 Pa
-3.50 kV
0.10 uA
1300 1500 1700
+0.0
+0.0
+0.0
+0.8
+0.8
+1.0
+5.0
+0.0
+5.0
+9.0
1900